344
Electroactive Materials Design Strategies Toward Increased Electrical Conductivity: Impact on Electrochemistry

Monday, 29 May 2017: 15:40
Grand Salon D - Section 21 (Hilton New Orleans Riverside)
A. C. Marschilok, E. S. Takeuchi, and K. J. Takeuchi (Stony Brook University)
Energy storage materials remain important due to their ability to store electricity for many applications including aerospace, transportation, portable electronics, and biomedical devices. Full utilization of materials requires fast transport of both ions and electrons to all regions of the electrode. Several approaches have been utilized to facilitate ion diffusion including dimension reduction, morphology control, and synthesis of layered and tunneled structures, however, electron access must also be considered. Low electrical conductivity can limit active material utilization, especially at high rates, and may be a cause of capacity fade.

One approach to address the low electrical conductivity of cathode materials is to utilize composite electrodes that contain conductive media, most often carbon. While commonly employed, this strategy is imperfect, as inhomogeneous dispersion of the active material in the conductive additive results in incomplete electrical contact to all particles in the electrode. Encapsulation of individual active material particles with a carbon coating can be more effective for providing electrical contact to each particle, however have the disadvantages of additional synthesis steps and increased production cost. An alternative strategy to approach an ideal electrode that we have been exploring is the use of bimetallic material systems. In this approach, the active material particles are electrically connected as they generate a conductive network in-situ on initiation of reduction. Bimetallic cathode materials offer the opportunity for conductive matrix formation via reduction displacement reactions that result in the formation of metal nanoparticles providing the electrical connections.

The investigation of bimetallic materials and the formation of electrically conductive pathways has included exploration of metal oxide and metal polyanion type structures including phosphate and diphosphate moieties. Additionally, composites containing bimetallic materials have been explored. The impact of this strategy on delivered capacity and capacity retention will be discussed.